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1 article(s) from De Vos, Dirk E

Electrocarboxylation: towards sustainable and efficient synthesis of valuable carboxylic acids

Roman Matthessen,
Jan Fransaer,
Koen Binnemans and
Dirk E. De Vos

Beilstein J. Org. Chem. 2014, 10, 2484–2500, doi:10.3762/bjoc.10.260

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Scheme 1: Synthesis of salicylic acid and p-hydroxybenzoic acid via Kolbe–Schmidt reaction [16-20].

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Scheme 2: Electroreduction of carbon dioxide to formic acid, methanol or methane.

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Scheme 3: Electrochemical fixation of CO₂ in olefins.

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Scheme 4: Electrohydrodimerisation of acrylonitrile to adiponitrile [32].

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Scheme 5: Parallel paired electrosynthesis of phthalide and tert-butylbenzaldehyde dimethylacetal [34].

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Scheme 6: Overview of electrocarboxylation setups using (a) a sacrificial anode, (b) an inert anode, generati...

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Scheme 7: General mechanism of the electrochemical dicarboxylation of conjugated dienes [49].

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Scheme 8: Reported anodic reactions for the electrocarboxylation of 1,3-butadiene.

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Scheme 9: General mechanism for electrocarboxylation of alkynes.

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Scheme 10: Electrocarboxylation of ethyl cinnamate [70].

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Scheme 11: General electrocarboxylation mechanism for carbonyl compounds (Y = O) and imines (Y = NH) [75-77].

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Scheme 12: Electrocarboxylation mechanism of butyraldehyde proposed by Doherty [78].

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Scheme 13: Electrocarboxylation of AMN to HN using a sacrificial aluminum anode [86].

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Scheme 14: Electrocarboxylation of benzalaniline using a sacrificial aluminum anode [105].

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Scheme 15: Electrocarboxylation of p-isobutylacetophenone with stable electrodes [94,95].

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Scheme 16: Electrochemical carboxylation of MMP to MHA [110,111].

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Scheme 17: General mechanism for electrocarboxylation of alkyl halides [122,124-126,128].

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Scheme 18: Electrocarboxylation of benzylic chlorides as synthesis route for NSAIDs.

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Scheme 19: Electrocarboxylation of 1,4-dibromo-2-butene [144].

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Scheme 20: Convergent paired electrosynthesis of cyanoacetic acid, with X⁻ = F₄B⁻, ClO₄⁻, HSO₄⁻, Cl⁻, Br⁻ [147].

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Scheme 21: General scheme of carboxylation of weak acidic hydrocarbons with electrogenerated bases. RH: weakly...

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Scheme 22: Electrocarboxylation of N-methyldiglycolimide to methoxymethane-1,1,1’-tricarboxylate precursors. R¹...

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Scheme 23: Electrochemical dimerization of CO₂ with stable electrodes [153].

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Review

Published 27 Oct 2014

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